By Sydney Marks
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Additional info for A textbook of inorganic chemistry vol.VI part III Vanadium, Niobium, and Tantalum
It is soluble in dichloromethane or liquid SO2,slightly soluble in carbon tetrachloride and THF, and insoluble in hydrocarbon solvents. Solid samples should be stored in a dry atmosphere. The characteristic IR absorptions of [N5S4]C1occur at 1140 (w), 1050 (s), 1023 (m), 966 (s), 800 (w), 720 (w), 697 (s), 628 (m), 584 (s) 560 (sh), 481 (m), 462 (m), 422 (m), 408 (m), 308 (w) cm-'. 3 x I@). References W. L. Jolly and K. D. Maguire, Inorg. , 9, 102 (1967). A. J. Banister and H. G. Clarke, Znorg.
E. Cordes, and F. A. , 35B, 980 (1979). 9. H. R. Allcock, Polyhedron, 6 , 119 (1987). 10. M. L. Nielson and G. Cranford, Inorg. , 6 , 94 (1960). 11. S. S. Krishnamurthy, A. C. Sau, A. R. Vasudeva Murthy, R. Keat, R. A. Shaw, and M. Woods, J . Chem. , 1976, 1405. 12. S. Krishnamurthy, A. C. Sau, and M. Woods, Advances in Inorganic and Radiochemistry, Vol. 21, H. J. Emeltus and A. G. ), Academic Press, New York, 1978, p. 41. 13. S. S. Krishnamurthy, A. C, Sau, A. R. Vasudeva Murthy, R. Keat, R. A.
The crystals are separated on a coarse glass frit by suction. 5H20in 20 mL of dilute hydrochloric acid is added with stirring. 8 For the precipitation of the ammonium hexachloroantimonate solution prepared in either way may be used directly without isolating the hexachloroantimonic acid hydrate. 26 Main Group Ring Systems and Related Compounds colorless crystalline precipitate of [NH4]SbC16is separated on a glass frit, washed with cold hydrochloric acid, and dried at 80" in an oil pump vacuum. 5 g (55%).
A textbook of inorganic chemistry vol.VI part III Vanadium, Niobium, and Tantalum by Sydney Marks