Get Analytical Profiles of Drug Substances, Vol. 1 PDF

By FLOREY KLAUS

ISBN-10: 0122608011

ISBN-13: 9780122608018

Profiles of Drug components, Excipients and similar technique vol 1. content material: entrance hide; Analytical Profiles of Drug ingredients, quantity 1; Copyright web page; Contents; AFFILIATIONS OF EDITORS, members, AND REVIEWERS; FOREWORD; PREFACE; bankruptcy 1. Acetohexamide; bankruptcy 2. Chlordiazepoxide; bankruptcy three. Chlordiazepoxide Hydrochloride; bankruptcy four. Cycloserine; bankruptcy five. Cyclothiazide; bankruptcy 6. Diazepam; bankruptcy 7. Erythromycin Estolate; bankruptcy eight. Halothane; bankruptcy nine. Levarterenol Bitartrate; bankruptcy 10. Meperidine Hydrochloride; bankruptcy eleven. Meprobamate; bankruptcy 12. Nortriptyline Hydrochloride; bankruptcy thirteen. Potassium Phenoxymethyl Penicillin. bankruptcy 14. Propoxyphene HydrochlorideChapter 15. Sodium Cephalothin; bankruptcy sixteen. Sodium Secobarbital; bankruptcy 17. Triamcinolone; bankruptcy 18. Triamcinolone Acetonide; bankruptcy 19. Triamcinolone Diacetate; bankruptcy 20. Vinblastine Sulfate; bankruptcy 21. Vincristine Sulfate. summary: Profiles of Drug components, Excipients and comparable method vol 1

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The range d e s c r i b e d i n USP X V I I I i s 212-218OC u s i n g Class I method 7. 7 D i f f e r e n t i a l Scanning C a l o r i m e t r y The DSC s p e c t r u m of c h l o r d i a z e p o x i d e h y d r o c h l o r i d e is shown i n F i g u r e 3. The exotherm observed a t 233°C c o r r e s p o n d s t o t h e m e l t i n g of t h e d r u g f o l l o w e d by decomp o s i t i o n a t a p p r o x i m a t e l y 241OC. 5 kcal/mole8. 8 Thermogravimetric A n a l y s i s A TGA scan performed on c h l o r d i a z e p o x i d e hydroc h l o r i d e e x h i b i t e d 90 l o s s of w e i g h t when h e a t e d t o 1O5OC8.

53 P h o t o m e t r i c S y s t e m References - 54 CYCLOSERINE 1. 1 Name, F o r z u l a , M o l e c u l a r W e i g h t Cycloserine is ~-4-amino-3isoxazolidone. ihite t o s l i g h t l y yellow, p r a c t i c a l l y o d o r l e s s c r y s t a l l i n e powder. 2. 1 I n f r a r e d Spectrum ':he i n f r a r e d spectrum of cycloserine p r e s e n t e d i n F i g . 1 was t a k e n i n a K B r p e l l e t . R s p e c t r u m o f t h e same s s m p l e t a k e n i n a N u j o l iiull is e s s e n t i a l l y i d e n t i c a l t o t h e one preserited.

300, 250 34. , e t a l . , Arch. , 296, 396 35. Beral, H . , e t a l . , Rev. 36. Grev. I . , a n d ' Barku, S . (1964). (1967). (1963). (1965). 199 (1968). 37 16,1 6 9 (Bucharest), 16, a i m . (Bucharest), , Farmacia CHLORDIAZEPOXIDE HYDROCHLORIDE A . MacDonald, A . F. Michaelis, and B. Z . Senkowski 39 A. MacDONALD, A. F. MICHAELIS, AND 6. 2 . SENKOWSKI CONTENTS Analytical Profile - Chlordiazepoxide Hydrochloride 1. 2 Appearance, C o l o r , Odor 2. 10 C r y s t a l P r o p e r t i e s 2 . 12 Distribution Coefficient* 3.

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Analytical Profiles of Drug Substances, Vol. 1 by FLOREY KLAUS


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